TA Instruments

AR1756-0007f

15/03/2013 15:01:53

Sample name	ASW Blank coupon#20 + DI + beads 275rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	7 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:01:53

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 275.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	274.1	-7311.4	10000	20.0	0.2230	1.008	-2383	342.6	-6.955	908.5	163.4930	7.739E-3	204.37	20437	3.411E-3	0.0	0.0
2.0240	275.0	580.87	10000	20.0	0.1944	2.024	189.3	343.7	0.5509	791.9	503.6910	6.704E-3	629.61	62961	3.411E-3	0.0	0.0
3.0200	275.0	577.78	10000	20.0	0.1840	3.020	188.3	343.7	0.5479	749.8	728.9890	6.346E-3	911.24	91124	3.411E-3	0.1	0.1
4.0200	275.0	581.71	10000	20.0	0.1842	4.020	189.6	343.7	0.5516	750.6	1069.7400	6.353E-3	1337.2	1.3372E5	3.411E-3	0.1	0.1
5.0080	275.0	571.48	10000	20.0	0.1783	5.008	186.3	343.8	0.5419	726.6	1295.5699	6.149E-3	1619.5	1.6195E5	3.411E-3	0.1	0.1
6.0200	275.0	569.35	10000	20.0	0.1745	6.020	185.6	343.7	0.5399	710.9	1635.3600	6.016E-3	2044.2	2.0442E5	3.411E-3	0.1	0.1
7.0240	275.0	565.29	10000	20.0	0.1798	7.024	184.3	343.8	0.5360	732.4	1862.2900	6.198E-3	2327.9	2.3279E5	3.411E-3	0.1	0.1
8.0200	275.0	564.68	10000	20.0	0.1775	8.020	184.1	343.8	0.5354	723.3	2202.2300	6.121E-3	2752.8	2.7528E5	3.411E-3	0.1	0.1
9.0200	275.0	559.08	10000	20.0	0.1800	9.020	182.2	343.8	0.5301	733.2	2428.6899	6.205E-3	3035.9	3.0359E5	3.411E-3	0.2	0.2
10.020	275.0	544.66	10000	20.0	0.1836	10.020	177.5	343.8	0.5164	748.1	2651.6001	6.330E-3	3314.5	3.3145E5	3.411E-3	0.2	0.2
11.024	275.0	553.19	10000	20.0	0.1824	11.024	180.3	343.8	0.5245	743.2	2990.9700	6.288E-3	3738.7	3.7387E5	3.411E-3	0.2	0.2
12.020	275.0	562.26	10000	20.0	0.1763	12.020	183.3	343.7	0.5332	718.4	3219.6599	6.080E-3	4024.6	4.0246E5	3.411E-3	0.2	0.2
13.020	275.0	537.44	10000	20.0	0.1802	13.020	175.2	343.8	0.5096	734.1	3556.3601	6.211E-3	4445.5	4.4455E5	3.411E-3	0.2	0.2
14.020	275.0	554.42	10000	20.0	0.1761	14.020	180.7	343.8	0.5257	717.5	3785.0801	6.072E-3	4731.4	4.7314E5	3.411E-3	0.2	0.2
15.020	275.0	578.81	10000	20.0	0.1769	15.020	188.7	343.8	0.5488	720.8	4123.2900	6.099E-3	5154.1	5.1541E5	3.411E-3	0.3	0.3
16.020	275.0	551.80	10000	20.0	0.1789	16.020	179.9	343.8	0.5232	729.1	4350.1802	6.170E-3	5437.7	5.4377E5	3.411E-3	0.3	0.3
17.020	275.0	546.11	10000	20.0	0.1818	17.020	178.0	343.8	0.5178	740.7	4574.3398	6.268E-3	5717.9	5.7179E5	3.411E-3	0.3	0.3
18.020	275.0	567.59	10000	20.0	0.1749	18.020	185.0	343.7	0.5382	712.6	4913.6299	6.030E-3	6142.0	6.1420E5	3.411E-3	0.3	0.3
19.020	275.0	548.98	10000	20.0	0.1808	19.020	178.9	343.7	0.5206	736.5	5139.8701	6.233E-3	6424.8	6.4248E5	3.411E-3	0.3	0.3
20.020	275.0	558.58	10000	20.0	0.1814	20.020	182.1	343.7	0.5297	739.0	5479.0000	6.255E-3	6848.8	6.8488E5	3.411E-3	0.3	0.3
21.016	275.0	548.93	10000	20.0	0.1800	21.016	178.9	343.8	0.5204	733.2	5706.9702	6.203E-3	7133.7	7.1337E5	3.411E-3	0.4	0.4
22.024	275.0	552.27	10000	20.0	0.1852	22.024	180.0	343.7	0.5237	754.7	6045.7700	6.388E-3	7557.2	7.5572E5	3.411E-3	0.4	0.4
23.020	275.0	553.82	10000	20.0	0.1798	23.020	180.5	343.8	0.5251	732.4	6273.2700	6.198E-3	7841.6	7.8416E5	3.411E-3	0.4	0.4
24.044	275.0	558.86	10000	20.0	0.1775	24.044	182.2	343.8	0.5299	723.3	6497.2100	6.121E-3	8121.5	8.1215E5	3.411E-3	0.4	0.4
25.020	275.0	557.25	10000	20.0	0.1810	25.020	181.6	343.8	0.5284	737.4	6836.3101	6.239E-3	8545.4	8.5454E5	3.411E-3	0.4	0.4
26.020	275.0	562.28	10000	20.0	0.1806	26.020	183.3	343.8	0.5332	735.7	7062.3799	6.226E-3	8828.0	8.8280E5	3.411E-3	0.4	0.4
27.020	275.0	561.17	10000	20.0	0.1781	27.020	182.9	343.8	0.5321	725.8	7405.1401	6.141E-3	9256.4	9.2564E5	3.411E-3	0.5	0.5
28.028	275.0	553.12	10000	20.0	0.1822	28.028	180.3	343.8	0.5245	742.3	7629.1401	6.282E-3	9536.4	9.5364E5	3.411E-3	0.5	0.5
29.024	275.0	560.66	10000	20.0	0.1761	29.024	182.7	343.7	0.5317	717.5	7968.3701	6.073E-3	9960.5	9.9605E5	3.411E-3	0.5	0.5
30.020	275.0	564.30	10000	20.0	0.1761	30.020	183.9	343.7	0.5351	717.5	8196.2100	6.073E-3	10245	1.0245E6	3.411E-3	0.5	0.5
31.020	275.0	563.35	10000	20.0	0.1706	31.020	183.6	343.7	0.5342	695.2	8419.7598	5.884E-3	10525	1.0525E6	3.411E-3	0.5	0.5
32.020	275.0	561.91	10000	20.0	0.1824	32.020	183.2	343.7	0.5329	743.2	8758.9502	6.291E-3	10949	1.0949E6	3.411E-3	0.5	0.5
33.028	275.0	545.72	10000	20.0	0.1773	33.028	177.9	343.7	0.5175	722.5	8985.1104	6.115E-3	11231	1.1231E6	3.411E-3	0.6	0.6
34.020	275.0	556.01	10000	20.0	0.1800	34.020	181.2	343.7	0.5273	733.2	9324.4004	6.206E-3	11656	1.1656E6	3.411E-3	0.6	0.6
35.024	275.0	543.31	10000	20.0	0.1818	35.024	177.1	343.8	0.5152	740.7	9550.5996	6.268E-3	11938	1.1938E6	3.411E-3	0.6	0.6
36.024	275.0	548.61	10000	20.0	0.1751	36.024	178.8	343.8	0.5202	713.4	9889.8398	6.037E-3	12362	1.2362E6	3.411E-3	0.6	0.6
37.024	275.0	565.99	10000	20.0	0.1704	37.024	184.5	343.8	0.5366	694.4	10117.400	5.875E-3	12647	1.2647E6	3.411E-3	0.6	0.6
38.028	275.0	550.52	10000	20.0	0.1787	38.028	179.4	343.7	0.5220	728.3	10342.300	6.164E-3	12928	1.2928E6	3.411E-3	0.6	0.6
39.000	275.0	558.33	10000	20.0	0.1763	39.000	182.0	343.7	0.5294	718.4	10683.000	6.080E-3	13354	1.3354E6	3.411E-3	0.7	0.7
40.024	275.0	563.60	10000	20.0	0.1729	40.024	183.7	343.7	0.5344	704.3	10907.900	5.961E-3	13635	1.3635E6	3.411E-3	0.7	0.7
41.024	275.0	545.99	10000	20.0	0.1743	41.024	178.0	343.7	0.5177	710.1	11249.200	6.010E-3	14062	1.4062E6	3.411E-3	0.7	0.7
42.020	275.0	558.18	10000	20.0	0.1739	42.020	181.9	343.8	0.5293	708.4	11473.300	5.995E-3	14342	1.4342E6	3.411E-3	0.7	0.7
43.028	275.0	561.51	10000	20.0	0.1779	43.028	183.0	343.7	0.5325	725.0	11815.800	6.136E-3	14770	1.4770E6	3.411E-3	0.7	0.7
44.020	275.0	556.30	10000	20.0	0.1749	44.020	181.3	343.7	0.5275	712.6	12042.200	6.031E-3	15053	1.5053E6	3.411E-3	0.7	0.7
45.024	275.0	554.79	10000	20.0	0.1802	45.024	180.8	343.8	0.5260	734.1	12265.100	6.212E-3	15331	1.5331E6	3.411E-3	0.8	0.8
46.020	275.0	549.54	10000	20.0	0.1796	46.020	179.1	343.7	0.5211	731.6	12604.300	6.191E-3	15755	1.5755E6	3.411E-3	0.8	0.8
47.004	275.0	554.82	10000	20.0	0.1755	47.004	180.8	343.7	0.5261	715.1	12830.600	6.052E-3	16038	1.6038E6	3.411E-3	0.8	0.8
48.028	275.0	550.39	10000	20.0	0.1806	48.028	179.4	343.8	0.5218	735.7	13169.800	6.225E-3	16462	1.6462E6	3.411E-3	0.8	0.8
49.020	275.0	560.44	10000	20.0	0.1775	49.020	182.7	343.7	0.5314	723.3	13396.100	6.121E-3	16745	1.6745E6	3.411E-3	0.8	0.8
50.020	275.0	558.18	10000	20.0	0.1798	50.020	181.9	343.7	0.5293	732.4	13737.300	6.199E-3	17172	1.7172E6	3.411E-3	0.8	0.8
51.004	275.0	564.67	10000	20.0	0.1796	51.004	184.1	343.8	0.5354	731.6	13963.200	6.191E-3	17454	1.7454E6	3.411E-3	0.9	0.9
52.004	275.0	555.13	10000	20.0	0.1802	52.004	180.9	343.8	0.5264	734.1	14188.400	6.212E-3	17736	1.7736E6	3.411E-3	0.9	0.9
53.020	275.0	554.67	10000	20.0	0.1753	53.020	180.8	343.8	0.5259	714.2	14528.100	6.043E-3	18160	1.8160E6	3.411E-3	0.9	0.9
54.020	275.0	573.17	10000	20.0	0.1743	54.020	186.8	343.7	0.5435	710.1	14753.100	6.010E-3	18441	1.8441E6	3.411E-3	0.9	0.9
55.004	275.0	563.49	10000	20.0	0.1814	55.004	183.7	343.7	0.5343	739.0	15097.000	6.255E-3	18871	1.8871E6	3.411E-3	0.9	0.9
56.016	275.0	556.90	10000	20.0	0.1812	56.016	181.5	343.7	0.5281	738.2	15318.500	6.248E-3	19148	1.9148E6	3.411E-3	0.9	0.9
57.024	275.0	557.38	10000	20.0	0.1798	57.024	181.7	343.7	0.5286	732.4	15657.900	6.199E-3	19572	1.9572E6	3.411E-3	1.0	1.0
58.028	275.0	565.43	10000	20.0	0.1773	58.028	184.3	343.7	0.5362	722.5	15884.900	6.115E-3	19856	1.9856E6	3.411E-3	1.0	1.0
59.020	275.0	557.61	10000	20.0	0.1792	59.020	181.8	343.7	0.5288	729.9	16224.400	6.178E-3	20281	2.0281E6	3.411E-3	1.0	1.0
60.032	275.0	558.49	10000	20.0	0.1771	60.032	182.0	343.7	0.5296	721.7	16451.900	6.108E-3	20565	2.0565E6	3.411E-3	1.0	1.0

